10. Preparation of nanocrystalline NiZnCu ferrite particles by Sol-gel method and their magnetic properties
作者：S. Yan, J. Geng, L. Yin, E. Zhou,*
關(guān)鍵字：Sol–gel method, Nanocrystalline, NiZnCu ferrite, Mossbauer spectroscopy, Magnetic properties
論文來源：期刊
具體來源：J. Magn. Magn. Mater. 2004, 277, 84-89
發(fā)表時間：2004年
Polyvinyl alcohol (PVA) was first used as chelating agent and metal nitrates as precursor of ferrite in the fabrication of nanocrystalline Ni0.65Zn0.35Cu0.1Fe1.9O4 particles by the sol–gel method. The thermal decomposition process of dried gel was studied by thermogravimetry (TG), differential thermal analysis (DTA) and infrared spectra (IR). The structural and magnetic properties of resultant particles were investigated by X-ray diffraction (XRD), transmission electron microscope (TEM), vibrating sample magnetometer (VSM) and M.ossbauer spectroscopy. The dependence of the decomposition of dried gel, the formation of spinel structured NiZnCu ferrite, the sizes of annealed particles, the saturation magnetization and coercivity of annealed particles on annealing temperature is presented.