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Surface modification of polyamide nanofiber membranes by polyurethane to simultaneously improve their mechanical strength and hydrophobicity for breathable and waterproof applications
來源:郝文濤副教授個人網站 發布日期:2019-12-26
作者:Wen Yang, Ran Li, Caiping Fang, Wentao Hao
關鍵字:Electrospun, Nanofiber membrane, Robust, Waterproof, Breathable
論文來源:期刊
具體來源:https://doi.org/10.1016/j.porgcoat.2019.02.012
發表時間:2019年

In this work, a simple method was proposed to fabricate robust, breathable and waterproof polymer nanofiber membranes. In a typical process, polyamide-6 (PA-6) electrospun membranes were immersed into polyurethane (PU)/DMF solutions for 24 h, and then taken out and dried. SEM results showed that PA-6 nanofibers in the membranes adhered to each other at the inter-fiber junction points. Moreover, the nanofibers were covered by a thin layer of PU, which was also proved by FTIR results. The DSC and WAXD results suggested that the PU had interacted with the PA-6 at molecular level. Through adhesion bonding, the PA-6 nanofiber membrane was interlinked into a huge network, leading to drastically increment in tensile strength of these membranes (357% that of the original value). Moreover, the PA-6 membranes achieved good waterproof ability after the PU solution treatment. The water contact angle was 135.8°, comparable to that of the poly(vinylidene fluoride) (PVDF) electrospun membrane or fluorinated PU/PU coelectrospun membrane. Interestingly, the PU solution treated PA-6 membranes preserved good breathability. It is a facile and scalable approach to fabricate the robust, breathable and waterproof polymer nanofiber membranes.


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